薄膜—電導(dǎo)率法總有機(jī)碳分析儀測(cè)量結(jié)果不確定度的評(píng)定

時(shí)間：2009/1/15

摘要目的：建立薄膜—電導(dǎo)率法總有機(jī)碳分析儀測(cè)量結(jié)果不確定度的評(píng)定方法。方法：分析了測(cè)量過(guò)程中不確定度的主要來(lái)源，即工作曲線(xiàn)的不確定度、測(cè)量?jī)x器讀數(shù)分辨率導(dǎo)致的不確定度、測(cè)量不重復(fù)性引起的不確定度、標(biāo)準(zhǔn)溶液引起的不確定度等，分別量化后合成標(biāo)準(zhǔn)不確定度，得到總有機(jī)碳測(cè)量的擴(kuò)展不確定度。結(jié)果：通過(guò)對(duì)HTY-2500總有機(jī)碳分析儀在2000μg·L^-1測(cè)量點(diǎn)測(cè)量結(jié)果不確定度的評(píng)定，其擴(kuò)展不確定度為U₉₅= 49（μg·L^-1）（k=2）。結(jié)論：本方法所建立的測(cè)量結(jié)果不確定度評(píng)定方法準(zhǔn)確、可靠，可為薄膜-電導(dǎo)率法總有機(jī)碳分析儀的測(cè)量結(jié)果不確定度評(píng)定提供較為準(zhǔn)確簡(jiǎn)便的方法。

關(guān)鍵詞：總有機(jī)碳；測(cè)量不確定度；薄膜—電導(dǎo)率法

中圖分類(lèi)號(hào)：R917 文獻(xiàn)標(biāo)識(shí)碼：A 文章編號(hào)：0254-1793（2008）12-0-0

Evaluation of Measurement Uncertainty for the Total Organic Carbon Analyzer with Membrane Conductmetric Detection Technology

YAN Xiang-qing¹，WU Xu-mei²

（1.Zhejiang Province Institute of Metrology, Hangzhou, 310013, China;2.Hangzhou Tailin Bioengineering Equipments Co. LTD, Hangzhou, 310052, China）

Abstract: Purpose: The article set up an evaluation method of measurement uncertainty for the total organic carbon analyzer with membrane conductmetric detection technology. Method: The article analyzed the main resources of the uncertainty of the measurement, which include uncertainty of the working curve, uncertainty of the resolution ratio of the instrument, uncertainty of measure unrepeatability, uncertainty of standard solution, etc. It quantified these uncertainties respectivelycomposed them to a standard uncertainty. Finally it got the expanded uncertainty of the total organic carbon measurement. Result: It evaluated the measurement uncertainty of the total organic carbon analyzer at 2000μg·L^-1got the expanded uncertainty which is U₉₅= 49（μg·L^-1）（k=2）. Conclusion: The evaluation method of measurement uncertainty set up by the article is accurate, reliable,it can offer comparatively exactconvenient method for measurement uncertainty evaluation of the total organic carbon analyzer with membrane conductmetric detection technology.

Key words: total organic carbon; uncertainty of a measurement; membrane-conductometric detection technology

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薄膜—電導(dǎo)率法總有機(jī)碳分析儀測(cè)量結(jié)果不確定度的評(píng)定

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